Crucible

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Skull Crucible.jpg

Origin

Middle English corusible, from Medieval Latin crucibulum earthen pot for melting metals

Definitions

  • 1: a vessel of a very refractory material (as porcelain) used for melting and calcining a substance that requires a high degree of heat
  • 2: a severe test
  • 3: a place or situation in which concentrated forces interact to cause or influence change or development <conditioned by having grown up within the crucible of Chinatown — Tom Wolfe>

Description

A crucible is a container that can withstand very high temperatures and is used for metal, glass, and pigment production as well as a number of modern laboratory processes. While crucibles historically were usually made from clay, they can be made from any material that withstands temperatures high enough to melt or otherwise alter its contents.

The form of the crucibles has varied through time, with designs reflecting the process for which they are used, as well as regional variation.The crucible helps to prevent the heat from affecting the solution. The earliest crucible forms derive from the sixth/fifth millennium B.C. in Eastern Europe and Iran.

Crucibles and their covers are made of high temperature-resistant materials, usually porcelain or an inert metal. One of the earliest uses of platinum was to make crucibles. Ceramics such as alumina, zirconia, and especially magnesia will tolerate the highest temperatures. More recently, metals such as nickel and zirconium have been used. The lids are typically loose-fitting to allow gases to escape during heating of a sample inside. Crucibles and their lids can come in high form and low form shapes and in various sizes, but rather small 10–15 ml size porcelain crucibles are commonly used for gravimetric chemical analysis. These small size crucibles and their covers made of porcelain are quite cheap when sold in quantity to laboratories, and the crucibles are sometimes disposed of after use in precise quantitative chemical analysis. There is usually a large mark-up when they are sold individually in hobby shops.[1]